Orbital - Vol. 11 No. 5 - July-September 2019
FULL PAPERS

Synthesis of Dibenzylidene Acetone via Aldol Condensation of Diacetone Alcohol with Substituted Benzaldehydes

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  • Pramod Kulkarni,
  • Ganesh Totre
Pramod Kulkarni
Post Graduate Centre in Organic Chemistry and Department of Chemistry, Hutatma Rajguru Mahavidyalaya, Rajgurunagar
Ganesh Totre
Post Graduate Centre in Organic Chemistry and Department of Chemistry, Hutatma Rajguru Mahavidyalaya, Rajgurunagar

Published 2019-10-04

Keywords

  • aldol condensation,
  • aromatic aldehyde,
  • calcium hydroxide,
  • diacetone alcohol,
  • dibenzylidene acetone
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How to Cite

(1)
Kulkarni, P.; Totre, G. Synthesis of Dibenzylidene Acetone via Aldol Condensation of Diacetone Alcohol With Substituted Benzaldehydes. Orbital: Electron. J. Chem. 2019, 11 (5), 292-296.

Abstract

Aldol condensation between diacetone alcohol and substituted benzaldehyde using calcium hydroxide as a base was investigated. Reaction of diacetone alcohol with benzaldehyde in the presence of base formed 4-benzylidene-5-hydroxy-5-methyl-1-phenylhex-1-en-3-one, which then converted into dibenzylidene acetone. The advantages of this method include high yield, use of inexpensive catalyst, easy workup, and simple purification process.

DOI: http://dx.doi.org/10.17807/orbital.v11i5.1388

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